;Juan A. Aguilar. Mathias Nilsson. Gareth A. Morris. Manchester. 2011. ;NB development version, subject to change. ;http://nmr.chemistry.manchester.ac.uk ;avance-version (30/11/2011) ;2D homonuclear shift correlation ;phase sensitive ;using gradient pulses for selection ;with multiple quantum filter according to gradient ratio ;constant time version ;$CLASS=HighRes ;$DIM=2D ;$TYPE= ;$SUBTYPE= ;$COMMENT= #include #include #include "p2=p1*2" "d13=4u" "in0=inf1/2" "in10=in0" "d0=d25-p16-d16" "d10=d25-p16-d16" "DELTA=p16+d16+d13" 1 ze 2 30m 10m UNBLKGRAD ;;;;;;;;;;;;;;;;;;;;; Pre-filter. Attenuation of rapid pulsing artefacts ;;;;;;;;;;; p16:gp0 d16 p1*500 ph11 10m p1*250 ph12 p16:gp0 ;;;;;;;;;;;;;;;;;;;;; Pre-filter. Attenuation of rapid pulsing artefacts ;;;;;;;;;;; d1 BLKGRAD ;;;;;;;;;;;;;;;;;;;;;;;;;;CT ;;;;;;;;;;;;;;;;;;;;;;;;;; 3 p1 ph1 d0 UNBLKGRAD p16:gp1 d16 p2 ph10 p16:gp1 d16 d10 ;;;;;;;;;;;;;;;;;;;;;;;;;;2Q ;;;;;;;;;;;;;;;;;;;;;;;;;; p1 ph2 DELTA p2 ph4 p16:gp2 d16 d13 ;;;;;;;;;;;;;;;;;;;;;;;;;;1Q ;;;;;;;;;;;;;;;;;;;;;;;;;; p1 ph3 DELTA p2 ph4 d13 p16:gp3 d16 BLKGRAD go=2 ph31 30m mc #0 to 2 F1PH(ip1, dd10 & id0) exit ph1=1 3 ph2=0 ph3=1 ph4=0 ph10=0 ph11=0 ph12=1 ph31=0 2 ;pl1 : f1 channel - power level for pulse (default) ;p1 : f1 channel - 90 degree high power pulse ;p2 : f1 channel - 180 degree high power pulse ;p16: homospoil/gradient pulse ;d0 : incremented delay (2D) ;d1 : relaxation delay; 1-5 * T1 ;d13: short delay [4 usec] ;d16: delay for homospoil/gradient recovery ;d25: d25*2.0 is the constant time. Make sure that td1/sw1/2 is longer than p16+d16. ;td1: number of experiments ;NS: 1 * n ;FnMODE: TPPI.;use gradient ratio: gp0 : gp1 : gp2 : gp3. ; -75 : 80 : -30 : 60 for a double quantum filter ; -75 : 80 : -15 : 45 for a triple quantum filter : The last two gradients form the n quantum filters. Use 1:2 for DQF, 1:3 for TQF, etc. ; The first gradient, gp0 is used to attenuate rapid pulsing artefacts. ; The second gradient, gp1, is used to clean up the 180 rf pulse of the constant time element. ;$Id: ber 05_d. Exp $