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A three-dimensional DOSY-HMQC experiment for the high-resolution analysis of complex mixtures

Mon, 03/14/2011 - 12:22 — ralph
TitleA three-dimensional DOSY-HMQC experiment for the high-resolution analysis of complex mixtures
Publication TypeJournal Article
Year of Publication1998
AuthorsBarjat, H, Morris GA, Swanson AG
JournalJournal of Magnetic Resonance
Volume131
Pagination131-138
ISBN Number1090-7807
Accession NumberWOS:000073133900017
Abstract

A three-dimensional experiment is described in which NMR signals are separated according to their proton chemical shift, C-13 chemical shift, and diffusion coefficient. The sequence is built up from a stimulated echo sequence with bipolar field gradient pulses and a conventional decoupled HMQC sequence, Results are presented for a model mixture of quinine, camphene, and geraniol in deuteriomethanol. (C) 1998 Academic Press.
URLhttp://apps.isiknowledge.com/UA_GeneralSearch_input.do?product=UA&search_mode=GeneralSearchWOS:000073133900017